Bleach 230 - 265 [Zampakutou Rebellion]

 Available Episodes ; 35
A group of Ryoka, led by a mysterious man, attacks Soul Society. Meanwhile, the Gotei 13 members feel a strange disturbance occurring within their Zanpakutō. The group of Ryoka first appears at the entrance to the 1st Division barracks. The first to encounter them are Vice-Captain Chōjirō Sasakibe and Captain-Commander Genryūsai Shigekuni Yamamoto. Immediately after the encounter, an emergency meeting is called by Captain Yamamoto at Sōkyoku Hill. Captain Kenpachi Zaraki would not attend, claiming that he was too bored. With all of the captains and vice-captains waiting for Yamamoto's appearance, Vice-Captain Chōjirō Sasakibe suddenly appears before them, collapsing in front of everyone.

A mysterious Ryoka, calling himself Muramasa, appears before them, claiming that Yamamoto would not be attending the meeting. An incensed Captain Sajin Komamura releases his Bankai, even while Muramasa claims that his Zanpakutō attacks will not work. When Komamura attacks anyway, Kokujō Tengen Myō'ō instead attacks its wielder. Confused, Komamura can only watch his Bankai disappear, just before Tenken's true form appears before him physically and attacks, causing him to collapse after losing a short battle.

Sumber: 
http://bleach.wikia.com/wiki/A_New_Enemy!_The_Materialization_of_Zanpakut%C5%8D
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